方法理论

基于核磁共振信号标定法的致密油藏渗吸实验研究

  • 唐慧莹 ,
  • 第凯翔 ,
  • 张烈辉 ,
  • 郭晶晶 ,
  • 张涛 ,
  • 田野 ,
  • 赵玉龙
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  • 西南石油大学油气藏地质及开发工程全国重点实验室,四川 成都 610500
唐慧莹(1990—),女,博士,副教授,主要从事非常规储层压裂及一体化数值模拟研究。地址:四川省成都市新都区新都大道8号西南石油大学,邮政编码:610500。E-mail: tanghuiying@swpu.edu.cn

收稿日期: 2023-10-30

  网络出版日期: 2024-07-10

基金资助

国家自然科学基金面上项目“井-射孔-缝协同密切割压裂三维非平面缝网竞争扩展机制研究”(52374043);国家自然科学基金重点项目“海相页岩水平井超临界二氧化碳压裂机理与一体化模拟研究”(52234003);国家自然科学基金青年基金“致密油藏基于化学势的多组分、多机理耦合扩散数值模拟方法研究”(52304048)

Tight oil imbibition based on nuclear magnetic resonance signal calibration method

  • Huiying TANG ,
  • Kaixiang DI ,
  • Liehui ZHANG ,
  • Jingjing GUO ,
  • Tao ZHANG ,
  • Ye TIAN ,
  • Yulong ZHAO
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  • State Key Laboratory of Oil and Gas Reservoir Geology and Exploitation, Southwest Petroleum University, Chengdu, Sichuan 610500, China

Received date: 2023-10-30

  Online published: 2024-07-10

摘要

基于一种新的核磁共振信号标定法开展了致密砂岩岩样的油水渗吸实验,该方法可以根据回归模型将核磁信号总量换算为含油体积,相较常规方法计算更方便、更准确。研究发现渗吸过程可划分为过渡渗吸和稳定渗吸2个阶段,低黏度煤油渗吸样品最佳渗吸时间集中在68 h左右,高黏度致密油渗吸样品最佳渗吸时间集中在188 h左右。渗吸时间充足的情况下,煤油和致密油的最终换油率相差不大,但如果渗吸时间较短,则黏度越大换油率越低。同层位、同黏度的样品具有相似的渗吸动态特征;同层位、高黏油的样品达到稳定渗吸阶段无因次渗吸时间相较低黏油更短。以半径0.5 μm作为大、小孔隙的分界线,煤油渗吸样品中半径小于0.5 μm的孔隙渗吸换油贡献率平均为83.93%,占据主导地位,原油动用率平均为23.54%;半径大于0.5 μm的孔隙渗吸换油贡献率平均为16.07%,相对较少,原油的动用率平均为8.50%,普遍较低,容易形成水锁。致密油渗吸样品在所有孔隙中的渗吸换油贡献率则相对均衡,半径小于0.5 μm的孔隙原油动用率平均为14.82%,相对较低;而半径大于0.5 μm的孔隙原油动用率平均为29.82%,在焖井过程中普遍会得到有效动用。

本文引用格式

唐慧莹 , 第凯翔 , 张烈辉 , 郭晶晶 , 张涛 , 田野 , 赵玉龙 . 基于核磁共振信号标定法的致密油藏渗吸实验研究[J]. 油气藏评价与开发, 2024 , 14(3) : 402 -413 . DOI: 10.13809/j.cnki.cn32-1825/te.2024.03.010

Abstract

This study explores oil-water imbibition dynamics in rock samples of tight sandstone with similar physical properties using a novel NMR signal calibration method. This method can translate the total NMR signal output into oil volume via a regression model, offering enhanced convenience and accuracy compared to traditional approaches. The imbibition process is characterized by two distinct phases: a rapid imbibition stage and a stable imbibition stage. Optimal imbibition times were identified as approximately 68 hours for oil from coal samples and 188 hours for tight oil samples. When imbibition times are sufficient, the recovery ratios for oil from coal and tight oil are comparable. However, with insufficient imbibition time, the recovery ratio for oil from coal is lower than that for tight oil. Within the same stratigraphic layer, samples with identical viscosity exhibit similar imbibition dynamics, with tight oil samples reaching the stable stage more quickly than oil from coal samples. The pivotal radius distinguishing large and small pores is established at 0.5 μm. In low-viscosity crude oil samples, small pores significantly dominate the imbibition process, contributing 83.93% to the recovery, while large pores contribute only 16.07%. The overall mobilization of crude oil is low at 8.50%, frequently resulting in the formation of water locks. In contrast, tight oil samples show a more balanced contribution across all pore sizes during the soaking period. The average utilization ratios of crude oil are 14.82% in small pores and 29.82% in large pores.

参考文献

[1] 邹才能, 杨智, 张国生, 等. 非常规油气地质学理论技术及实践[J]. 地球科学, 2023, 48(6): 2376-2397.
[1] ZOU Caineng, YANG Zhi, ZHANG Guosheng, et al. Theory, Technology and practice of unconventional petroleum geology[J]. Earth Science, 2023, 48(6): 2376-2397.
[2] 李昊远, 庞强, 魏克颖, 等. 致密砂岩储层孔隙结构分形特征对气水渗流规律的影响——以苏里格气田东南部桃2区块山1段为例[J]. 断块油气田, 2023, 30(2): 177-185.
[2] LI Haoyuan, PANG Qiang, WEI Keying, et al. Influence of pore structure fractal features of tight sandstone reservoir on gas-water seepage law: A case study of Shan 1 Member in Tao 2 block of southeastern Sulige Gas Field[J]. Fault-Block Oil & Gas Field, 2023, 30(2): 177-185.
[3] 徐二社, 黄娟, 鹿坤, 等. 致密油运聚动力研究:以渤海湾盆地东濮凹陷Wg4井沙三中致密油为例[J]. 断块油气田, 2023, 30(1): 17-24.
[3] XU Ershe, HUANG Juan, LU Kun, et al. The driving force study of tight oil migration and accumulation: A case study of the tight oil in Es32 Formation in well Wg4 of Dongpu Sag, Bohai Bay Basin[J]. Fault-Block Oil & Gas Field, 2023, 30(1): 17-24.
[4] 陈军军, 杨兴利, 高月, 等. 安塞油田坪桥区长6致密油储层微观特征[J]. 石油地质与工程, 2022, 36(5): 35-40.
[4] CHEN Junjun, YANG Xingli, GAO Yue, et al. Microstructure characteristics of Chang 6 tight sandstone reservoirs in Pingqiao area, Ansai oilfield, Ordos basin[J]. Petroleum Geology & Engineering, 2022, 36(5): 35-40.
[5] 吴云飞, 刘成林, 冯小龙, 等. 致密砂岩储层微观结构特征及分类评价——以鄂尔多斯盆地南梁油田长9储层为例[J]. 断块油气田, 2023, 30(2): 246-253.
[5] WU Yunfei, LIU Chenglin, FENG Xiaolong, et al. Microstructural characteristics and classification evaluation of tight sandstone reservoirs: a case study of the Chang 9 reservoir in the Nanliang Oilfield of the Ordos Basin[J]. Fault-Block Oil & Gas Field, 2023, 30(2): 246-253.
[6] GHANBARI E, ABBASI M A, DEHGHANPOUR H, et al. Flowback volumetric and chemical analysis for evaluating load recovery and its impact on early-time production[C] Paper SPE-167165-MS presented at the SPE Unconventional Resources Conference Canada, Calgary, Alberta, Canada, November 2013.
[7] GHANBARI E, DEHGHANPOUR H. The fate of fracturing water: A field and simulation study[J]. Fuel, 2016, 163: 282-294.
[8] 刘小明. 大庆油田致密油水平井体积改造技术发展与建议[J]. 石油地质与工程, 2023, 37(4): 108-112.
[8] LIU Xiaoming. Development and suggestions for volume transformation of tight oil by horizontal wells in Daqing Oilfield[J]. Petroleum Geology & Engineering, 2023, 37(4): 108-112.
[9] 蒋艳芳. 鄂尔多斯盆地致密油藏水平井二次压裂技术研究[J]. 石油地质与工程, 2022, 36(2): 93-95.
[9] JIANG Yanfang. Research of secondary fracturing technology for horizontal wells in tight reservoirs in Ordos Basin[J]. Petroleum Geology & Engineering, 2022, 36(2): 93-95.
[10] BROWNSCOMBE E R, DYES A B. Water-imbibition displacement: A possibility for the Spraberry[C]// Paper presented at the Drilling and Production Practice Conference, Chicago, Illinois, November.
[11] MAKHANOV K, HABIBI A, DEHGHANPOUR H, et al. Liquid uptake of gas shales: A workflow to estimate water loss during shut-in periods after fracturing operations[J]. Journal of Unconventional Oil and Gas Resources, 2014, 7(2): 22-32.
[12] 孙志成, 王贤君. 大庆油田致密油藏压裂返排液复配影响因素分析[J]. 石油地质与工程, 2023, 37(2): 97-101.
[12] SUN Zhicheng, WANG Xianjun. Analysis of influencing factors of fracturing flowback fluid compounding in tight reservoirs of Daqing Oilfield[J]. Petroleum Geology & Engineering, 2023, 37(2): 97-101.
[13] CHENG Y M. Impact of water dynamics in fractures on the performance of hydraulically fractured wells in gas-shale reservoirs[J]. Journal of Canadian Petroleum Technology, 2012, 51(2): 143-151.
[14] HABIBI A, DEHGHANPOUR H, BINAZADEH M, et al. Advances in understanding wettability of tight oil formations: A Montney case study[J]. SPE Reservoir Evaluation & Engineering, 2016, 19(4): 583-603.
[15] 贺东旭. 低渗致密油藏重复压裂用渗吸液的研究与应用[J]. 石油与天然气化工, 2023, 52(2): 99-103.
[15] HE Dongxu. Research and application of re-fracturing with imbibition technology in low permeability and tight oil reservoir[J]. Chemical Engineering of Oil & Gas, 2023, 52(2): 99-103.
[16] DENNEY D. Countercurrent imbibition processes in diatomite[J]. Journal of Petroleum Technology, 2015, 53(10): 44.
[17] 李士奎, 刘卫东, 张海琴, 等. 低渗透油藏自发渗吸驱油实验研究[J]. 石油学报. 2007, 28(2): 109-112
[17] LI Shikui, LIU Weidong, ZHANG Haiqin, et al. Experimental study of spontaneous imbibition in low-permeability reservoir[J]. Acta Petrolei Sinica, 2007, 28(2): 109-112
[18] ZHOU Z, HOFFMAN B T, BEARINGER D, et al. Experimental and numerical study on spontaneous imbibition of fracturing fluids in shale gas formation[J]. SPE Drilling & Completion, 2016, 31(3): 168-177.
[19] 钟家峻, 杨小军, 陈燕虎, 等. 低渗透岩心自然渗吸实验新方法[J]. 石油化工应用, 2013, 2(6): 61-65.
[19] ZHONG Jiajun, YANG Xiaojun, CHEN Yanhu, et al. The new experimental way of spontaneous imbibition in low-permeability cores[J]. Petrochemical Industry Application, 2013, 2(6): 61-65.
[20] 蒋卫东, 晏军, 杨正明. 火山岩气藏气水动态渗吸效率研究新方法[J]. 中国石油大学学报(自然科学版), 2012, 36(1): 101-105.
[20] JIANG Weidong, YAN Jun, YANG Zhengming. A new method of researching gas-water dynamic imbibition efficiency in volcanic gas reservoir[J]. Journal of China University of Petroleum(Edition of Natural Science), 2012, 36(1): 101-105.
[21] STAROV V M. Surfactant solutions and porous substrates: spreading and imbibition[J]. Advances in Colloid & Interface Science, 2004, 111(1-2): 3-27.
[22] CHAHARDOWLI M, ZHOLDYBAYEVA A, FARAJZADEH R, et al. Solvent-enhanced spontaneous imbibition infractured reservoirs[C]// Paper SPE-164908-MS presented at the EAGE Annual Conference & Exhibition incorporating SPE Europec, London, UK, June 2013.
[23] SHEHATA A M, NASR-EL-DIN H A. Spontaneous imbibition study: Effect of connate water composition on low-salinity waterflooding in sandstone reservoirs[C]// Paper SPE-174063-MS presented at the SPE Western Regional Meeting, Garden Grove, California, USA, April 2015.
[24] KATHEL P, MOHANTY K K. EOR in tight oil reservoirs through wettability alteration[C]// Paper SPE-166281-MS presented at the SPE Annual Technical Conference and Exhibition, New Orleans, Louisiana, USA, September 2013.
[25] 许建红, 马丽丽. 低渗透裂缝性油藏自发渗吸渗流作用[J]. 油气地质与采收率, 2015, 22(3): 111-114.
[25] XU Jianhong, MA Lili. Spontaneous imbibition in fractured low permeability reservoir[J]. Petroleum Geology and Recovery Efficiency, 2015, 22(3): 111-114.
[26] OLAFUYI O A, CINAR Y, KNACKSTEDT M A, et al. Spontaneous imbibition in small cores[C]// Paper SPE-109724-MS presented at the Asia Pacific Oil and Gas Conference and Exhibition, Jakarta, Indonesia, October 2007.
[27] LI K W, HORNE R N. Extracting capillary pressure and global mobility from spontaneous imbibition data in oil-water-rock systems[C]// Paper SPE-80553-MS presented at the SPE Asia Pacific Oil and Gas Conference and Exhibition, Jakarta, Indonesia, September 2003.
[28] LIU J R, SHENG J J. Experimental investigation of surfactant enhanced spontaneous imbibition in Chinese shale oil reservoirs using NMR tests[J]. Journal of Industrial and Engineering Chemistry, 2019, 72: 414-422.
[29] LIU J R, SHENG J J, WANG X K, et al. Experimental study of wettability alteration and spontaneous imbibition in Chinese shale oil reservoirs using anionic and nonionic surfactants[J]. Journal of Petroleum Science and Engineering, 2019, 175(2): 624-633.
[30] REZAVEISI M, AYATOLLAHI S, ROSTAMI B. Experimental investigation of matrix wettability effects on water imbibition in fractured artificial porous media[J]. Journal of Petroleum Science and Engineering, 2012, 86-87: 165-171.
[31] 王家禄, 刘玉章, 陈茂谦, 等. 低渗透油藏裂缝动态渗吸机理实验研究[J]. 石油探与开发, 2009, 36(1): 86-90.
[31] WANG Jialu, LIU Yuzhang, CHEN Maoqian, et al. Experimental study on dynamic imbibition mechanism of low permeability reservoirs[J]. Petroleum Exploration and Development, 2009, 36(1): 86-90.
[32] 杨正明, 朱维耀, 陈权, 等. 低渗透裂缝性砂岩油藏渗吸机理及其数学模型[J]. 石油天然气学报, 2001, 23(增刊1): 25-27.
[32] YANG Zhengming, ZHU Weiyao, CHEN Quan, et al. Imbibition mechanism of low permeability fractured sandstone reservoir and its mathematical model[J]. Journal of Oil and Gas Technology, 2001, 23(suppl. 1): 25-27.
[33] 杨正明, 刘学伟, 李海波, 等. 致密储集层渗吸影响因素分析与渗吸作用效果评价[J]. 石油勘探与开发, 2019, 46(4): 739-745.
[33] YANG Zhengming, LIU Xuewei, LI Haibo, et al. Analysis on the influencing factors of imbibition and the effect evaluation of imbibition in tight reservoirs[J]. Petroleum Exploration and Development, 2019, 46(4): 739-745.
[34] 刘长利, 刘欣, 张莉娜, 等. 裂缝性特低渗油藏渗吸效果影响因素实验研究[J]. 辽宁石油化工大学学报, 2017, 37(3): 35-38.
[34] LIU Changli, LIU Xin, ZHANG Lina, et al. Experimented study on the influence factors of spontaneous imbibition in ultra low permeability fractured reservoir[J]. Journal of Liaoning Petrochemical University, 2017, 37(3): 35-38.
[35] 朱维耀, 鞠岩, 赵明, 等. 低渗透裂缝性砂岩油藏多孔介质渗吸机理研究[J]. 石油学报, 2002, 23(6): 56-59.
[35] ZHU Weiyao, JU Yan, ZHAO Ming, et al. Spontaneous imbibition mechanisms of flow through porous media and waterflooding in low-permeability fractured sandstone reservoirs[J]. Acta Petrolei Sinica, 2002, 23(6): 56-59.
[36] 刘敦卿. 页岩储层微观渗吸效应及其对油气产出的影响[D]. 北京: 中国石油大学(北京), 2021.
[36] LIU Dunqing. Microscopic imbibition effects in shale reservoir and its impact on production[D]. Beijing: China University of Petroleum(Beijing), 2021.
[37] 冯绪宝. 页岩油油藏渗吸提高采收率实验研究[D]. 青岛: 中国石油大学(华东), 2020.
[37] FENG Xubao. Experimental study on enhancing oil recovery by imbibition in shale oil reservoir[D]. Qingdao: China University of Petroleum(East China), 2020.
[38] 杨坤. 裂缝性致密砂岩油藏渗吸规律及其影响因素研究[D]. 北京: 中国石油大学(北京), 2020.
[38] YANG Kun. Research on imbibition law of fractured tight sandstone reservoir and its influencing factors[D]. Beijing: China University of Petroleum(Beijing), 2020.
[39] MASON G, FISCHER H, MORROW N R, et al. Correlation for the effect of fluid viscosities on counter-current spontaneous imbibition[J]. Journal of Petroleum Science & Engineering, 2010, 72(1): 195-205.
[40] 龚小平, 唐洪明, 赵峰, 等. 四川盆地龙马溪组页岩储层孔隙结构的定量表征[J]. 岩性油气藏, 2016, 28(3): 48-57.
[40] GONG Xiaoping, TANG Hongming, ZHAO Feng, et al. Quantitative characterization of pore structure in shale reservoir of Longmaxi Formation in Sichuan Basin[J]. Lithologic Reservoirs, 2016, 28(3): 48-57.
[41] 程志林. 致密油砂岩渗吸实验及孔隙尺度模拟研究[D]. 北京: 中国石油大学(北京), 2021.
[41] CHENG Zhilin. Investigation on counter-current spontaneous imbibition in tight oil sandstones by experiments and pore scale simulation[D]. Beijing: China University of Petroleum(Beijing), 2021.
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